A. B. M. Shamsur Rahman, Herbert Boller, Kurt O. Klepp,
"Synthesis and Structural Characterization of [Me4N]2[W2O2(m-S)(h2-S2)4].MeCN a novel oxo-thiotungstate(VI)"
, in Zeitschrift für Naturforschung B: A Journal of Chemical Sciences, Vol. 54, Nummer 10, Seite(n) 1318-1322, 1999, ISSN: 0932-0776, A.B.M. Shamsur Rahman, H. Boller, K.O. Klepp: Synthesis and Structural Characterization of [Me4N]2[W2O2(m-S)(h2-S2)4].MeCN a novel oxo-thiotungstate(VI), Z. Naturforsch. 54b(1999) 1318-1322
Original Titel:
Synthesis and Structural Characterization of [Me4N]2[W2O2(m-S)(h2-S2)4].MeCN a novel oxo-thiotungstate(VI)
Sprache des Titels:
Englisch
Original Kurzfassung:
Orange red crystals of the new compound [Me4N]2[W2O2(?-S2)(eta2-S2)4].MeCN were obtained from the reaction of a solution of [Me4N]2[WOS3]in MeCN with solid AuCN at room temperature. They are monoclinic, space group P21/n, with a=9.264(2), b=17.736(3), c=18.742(5)Ä, beta=95.19(1)?; Z=4. The crystal structure was determined from single crystal diffractometer data (MoKalpha-radiation) and refined to R=0.050 (2955 reflections, 221 variable parameters). It is characterized by binuclear complex anions
Sprache der Kurzfassung:
Englisch
Journal:
Zeitschrift für Naturforschung B: A Journal of Chemical Sciences
Volume:
54
Number:
10
Seitenreferenz:
1318-1322
Erscheinungsjahr:
1999
Notiz zum Zitat:
A.B.M. Shamsur Rahman, H. Boller, K.O. Klepp: Synthesis and Structural Characterization of [Me4N]2[W2O2(m-S)(h2-S2)4].MeCN a novel oxo-thiotungstate(VI), Z. Naturforsch. 54b(1999) 1318-1322